PeptideMeter result on a Tianjin liraglutide lot lands 4.0 points below the supplier’s figure
A reminder that a purity figure is the output of a method, and that methods differ.
TheCompound Journal
Reporting on incretins, compounding & the peptide supply chain
Page 5 of 27 of this archive, newest first.
A reminder that a purity figure is the output of a method, and that methods differ.
A reminder that a purity figure is the output of a method, and that methods differ.
What happens to traceability when bulk material is subdivided, repackaged and relabelled two or three times before sale.
A manufacturer’s certificate is a self-declaration. An accredited laboratory’s report is a third-party measurement. The trade prints both under one heading.
The Journal submitted the sample and paid for the analysis. The vendor was told in advance.
The Journal submitted the sample and paid for the analysis. The vendor was told in advance.
The Journal submitted the sample and paid for the analysis. The vendor was told in advance.
Two years ago we ran an anonymised version of this comparison and promised a named one. This is it, with every method printed in full.
The Journal submitted the sample and paid for the analysis. The vendor was told in advance.
A badge asserts that something was tested. It does not assert what, when, on whose sample, by what method, or whether the lot on sale is the lot that was tested.
The report states the gradient, the wavelength and the integration threshold, which is more than most.
Two years ago we ran an anonymised version of this comparison and promised a named one. This is it, with every method printed in full.
We asked all four services what they can determine, on what timescale, at what price, and under what accreditation. The answers are printed in full.
Accreditation is granted for a defined scope of methods. A laboratory can be properly accredited and the test on your certificate can sit outside it.
The condition on arrival is recorded by some services and not others, and it is one of the more informative lines in a report.
The Journal’s standing position: a mass that matches is necessary evidence of identity and nowhere near sufficient.
Every step between the laboratory report and the product page removes information, and the badge is the last step.
The Journal has read several hundred certificates from twenty companies. We set out what the documents actually cover, and what a reader is filling in from imagination.
A document is only as good as the chain that connects it to the material, and most chains here are two or three links longer than the paperwork admits.
System suitability is the set of checks demonstrating that the instrument and method were performing adequately when your sample was injected. It is recorded as a matter of…